Improved conditions for the synthesis of tertiary fluorides using a KF/H2SO4 combination - Université de Bordeaux
Article Dans Une Revue Journal of Fluorine Chemistry Année : 2024

Improved conditions for the synthesis of tertiary fluorides using a KF/H2SO4 combination

Résumé

In this paper, we report the deoxyfluorination of tertiary alcohol using a simple combination of potassium fluoride and sulfuric acid. These cheap and widely available reagents allow for the synthesis of tertiary fluorides in good to excellent yields. Extension of the reaction to other functional groups such as alkenes, acetates and ethers have also been studied.
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Dates et versions

hal-04750598 , version 1 (23-10-2024)

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Xavier Bertrand, Doria Aissaoui, Océane Meryem Col, Laurent Chabaud, Jean-François Paquin, et al.. Improved conditions for the synthesis of tertiary fluorides using a KF/H2SO4 combination. Journal of Fluorine Chemistry, 2024, 279, pp.110338. ⟨10.1016/j.jfluchem.2024.110338⟩. ⟨hal-04750598⟩
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